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Outside of Gyarados, my first was a shiny Spearow in Gold. After beating the game, I was sad since my brother had found a shiny Zubat on his Silver in Union Cave on the same day he started his journey and I had found none, so I actually went hunting for a shiny at the base of Route 46 one morning. After five or so battles, out came a shiny Spearow at level 2. I was so happy...
I actually recreated my shiny Fearow in Black as an RNG Egg project, with the Sniper ability and a Jolly nature. I haven't used her in a battle yet, but I'm still quite fond of her...
The only shiny I've ever found was in Diamond. It was in the silent spring or whatever the lake that Giratina lives by is called. It was pretty exciting since it was my first non Red Gyarados shiny, and it was... Gyarados. -___-
Zubat (several times troughout different versions ... god i hate them)
Soul Silver: Koffing .. actually damn cool as shiny but its nature sucks ... i still have it in my team though (like i said it's pretty cool and not 'totally' useless). ... and a Drowzee ... wow that thing sucked so badly :-/
Hey i'm not camping ... i'm "tactically waiting" :-D